LI Ji, TANG Liying, ZHOU Rongcan, et al. Investigation on the precipitation characteristics and electrochemical responsibility of Laves phase during internal pressure creep test of T92[J]. Thermal power generation, 2023, 52(8): 96-103.
LI Ji, TANG Liying, ZHOU Rongcan, et al. Investigation on the precipitation characteristics and electrochemical responsibility of Laves phase during internal pressure creep test of T92[J]. Thermal power generation, 2023, 52(8): 96-103. DOI: 10.19666/j.rlfd.202212217.
In order to well evaluate the availability of electrochemical method using to detect the creep damage of martensitic heat resistant steel
a set of T92 internal pressure creep test samples with different creep damage degrees were selected. The microstructure evolution in the process of creep
especially the Laves phase precipitation behavior
was systematically characterized and analyzed; meanwhile
electrochemical response of Laves phase in alkaline were also investigated in detail. According to the scanning electron microscopy(SEM)
transmission electron microscopy(TEM) and electron probe X-ray micro-analyzer(EPMA) results
the Laves phase in T92 precipitated and grew rapidly during the internal pressure creep process. Its particle size and area percentage gradually increased
clustered and with element segregated and redistributed. According to potentiodynamic polarization curve in NaOH solution
Laves phase can selectively dissolve in strong alkali solution. When the concentration of NaOH reaches 8 mol/L
the current peak and corresponding electric value of selective dissolution of Laves phase are well correlated with the internal pressure creep time. In conclusion
the potentiodynamic polarization curve of T92 in strongly alkaline solution can effectively reflect the content of Laves phase
varying in consistent with its electric quantity; and can further associate with creep life damage. It is promising to be used as a nondestructive testing technology for the creep life assessment of pipelines in the field.