Synthesis of Pure Hexagonal Copper Sulfide Micro-crystals with Symmetric Concaved Polyhedrons by Ethanol Solvothermal Method

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- Synthesis of Pure Hexagonal Copper Sulfide Micro-crystals with Symmetric Concaved Polyhedrons by Ethanol Solvothermal Method
- Vol. 33, Issue 3, Pages: 93-96(2016)
- 作者机构：
- 作者简介：
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- DOI：10.3969/j.issn.1007-7162.2016.03.017
  CLC：
- Online First：19 May 2016，
  
  Published：2016
- 稿件说明：
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曾丽珍, 赵少飞. 对称性凹多面体六方相CuS微晶的溶剂热法制备研究[J]. 广东工业大学学报, 2016, 33(3): 93-96.

Zeng Li-zhen, Zhao Shao-fei. Synthesis of Pure Hexagonal Copper Sulfide Micro-crystals with Symmetric Concaved Polyhedrons by Ethanol Solvothermal Method[J]. 2016, 33(3): 93-96.
曾丽珍, 赵少飞. 对称性凹多面体六方相CuS微晶的溶剂热法制备研究[J]. 广东工业大学学报, 2016, 33(3): 93-96. DOI： 10.3969/j.issn.1007-7162.2016.03.017.

Zeng Li-zhen, Zhao Shao-fei. Synthesis of Pure Hexagonal Copper Sulfide Micro-crystals with Symmetric Concaved Polyhedrons by Ethanol Solvothermal Method[J]. 2016, 33(3): 93-96. DOI： 10.3969/j.issn.1007-7162.2016.03.017.

用CuSO

为铜源，硫粉为硫源，无水乙醇为溶剂，在180 ℃，反应12 h，用溶剂热法制备了由纳米片自组装对称的凹多面体CuS微晶.用X射线粉末衍射仪（XRD）、场发射扫描电子显微镜（FESEM）、透射电镜（TEM）及选区电子衍射（SAED）等对产物的成分、形状和尺寸进行了表征分析.结果表明

CuS微晶具有对称性凹多面体结构，该方法操作简单，反应条件温和并且有较高的重复性和可控性，是合成材料的一种有效方法.

Pure hexagonal copper sulfide micro-crystals with symmetric concaved polyhedrons were synthesized by ethanol solvothermal method and using CuSO

and S as raw materials

ethanol as solvent. The reaction was processed at 180 ℃ for 12 h. The composition

shape and size of synthetic copper sulfide micro-crystals are characterized by the equipments of XRD

FESEM

TEM and SAED. The result reveals that the copper sulfide crystals are symmetric concaved polyhedrons. It is a simple

gentle and effective synthesis method for micro-crystals materials.

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