YI Shu-fan, ZHANG Ya-hui, LI Chang-dong, et al. Micromechanical properties of key rock-forming minerals based on nanoindentation[J]. 2025, 46(12): 3841-3854+3912.
DOI:
YI Shu-fan, ZHANG Ya-hui, LI Chang-dong, et al. Micromechanical properties of key rock-forming minerals based on nanoindentation[J]. 2025, 46(12): 3841-3854+3912.DOI: 10.16285/j.rsm.2025.0008.
Micromechanical properties of key rock-forming minerals based on nanoindentation
Laboratory testing has become the most direct and accurate method for determining the mechanical properties of rocks. The mineral-rock multiscale analysis technology
using digital core modeling and discrete element simulation
reveals the regulatory mechanism of microscopic mineral mechanical parameters on macroscopic engineering responses
providing a theoretical tool for the assessment and prevention of geological disasters. Nanoindentation is an important technique for studying micromechanics
and current nanoindentation studies on rocks focus mainly on shale and granite; few studies address basalt
gneiss
schist
slate
or other rocks
and little is known about whether the same rock-forming mineral exhibits different micromechanical properties across rocks. In this study
the compositions
contents
apparent morphology and micromechanical properties of the main rock-forming minerals in ten categories of rocks are obtained by means of powder X-ray diffraction test
optical microscope surface observation
electron probe test and nanoindentation test
and the suitable peak loads of different rock-forming minerals for nanoindentation test are selected experimentally. A large body of literature on nanoindentation is compiled to compare the micromechanical properties of the same mineral across rocks and to reveal underlying causes. The indentation results indicate a significant linear relationship between fracture toughness and the elastic modulus; the relationship with hardness is not statistically significant. The appropriate peak load for quartz
potassium feldspar and plagioclase is 7 mN
that for mica is 3 mN
and that for calcite and dolomite is 4 mN. Nanoindentation curves differ substantially among minerals. Quartz data show the least dispersion
followed by potassium feldspar; plagioclase
dolomite
and calcite exhibit moderate dispersion. Compared with published studies
the granite data show strong concordance; for other rocks
the results can guide the selection of nanoindentation parameters. This further provides a basis for parametric modeling of rocks from the perspective of micro-mechanical properties
which is of great significance for studying the micro-macro mechanical behavior of rocks. In addition
in combination with environmental geology and sustainable development needs
multi-scale analysis technology can reveal the mechanical response mechanism of minerals and rocks in complex environments
further expanding its application prospects in the development of new energy materials and ecological restoration engineering.