ZHANG Chun-rui, JI Hong-guang, FU Zhen, et al. Influence of dolomite on the physical and mechanical properties of siltstone[J]. 2025, 46(9): 2661-2675.
DOI:
ZHANG Chun-rui, JI Hong-guang, FU Zhen, et al. Influence of dolomite on the physical and mechanical properties of siltstone[J]. 2025, 46(9): 2661-2675.DOI: 10.16285/j.rsm.2024.1378.
Influence of dolomite on the physical and mechanical properties of siltstone
白云石是通过白云石化作用形成,该过程使岩石孔隙率增加,以白云石为特征矿物,研究其对粉砂岩物理力学性能劣化的影响,对深部地下工程设计和稳定性预测具有重要意义。基于X射线荧光光谱仪(X-ray fluorescence spectrometer,简称XRF)、X射线衍射仪(X-ray diffractometer,简称XRD)、镜下鉴定、超声波波速、核磁共振测试,定量分析了白云石对粉砂岩物理参数的影响;通过巴西劈裂、单调加载、循环加卸载试验,获得了抗拉强度、抗压强度等力学参数的演化规律;建立了表观弹−黏−塑损伤模型,结合计算机断层扫描(computerized tomography,简称CT)和扫描电子显微镜(scanning electron microscope,简称SEM)扫描探究了白云石诱发粉砂岩劣化的机制。结果表明:(1)白云石的存在使颗粒磨圆度优,晶间咬合程度弱,与方解石交代边界孔隙明显,使孔隙连通性提升,孔隙率增大了2.77倍。(2)白云石的存在使抗拉最大应变减小,使抗压强度折减了14.5%,压密阶段延长了9%,裂纹稳定扩展阶段缩短了12%。(3)循环加卸载应力差值越大损伤值越高,不含白云石的岩石损伤变化较大,呈前期快速增加,后期缓慢增加的趋势,而含白云石的岩石损伤变化较为平稳,白云石使表观弹−黏−塑性损伤积累更剧烈。(4)不含白云石岩样裂纹弯折,耗散能较高,蓄能值低,含白云石岩样裂纹平直,耗散能较低,蓄能值高。白云石的存在使孔隙连通性增强,裂纹更易扩展,张拉裂纹占比升高。
Abstract
Dolomite is formed via dolomitization
a process that enhances porosity. Investigating the influence of dolomite as a characteristic mineral on the deterioration of the physical and mechanical properties of siltstone is significant for the design and stability prediction of deep underground engineering. This study employs X-ray fluorescence spectrometer (XRF)
X-ray diffraction (XRD)
microscopic analysis
ultrasonic wave velocity measurements
and nuclear magnetic resonance testing to quantify dolomite’s impact on siltstone’s physical parameters. Brazilian splitting tests
monotonic loading
and cyclic loading-unloading experiments reveal the evolution of mechanical parameters
including tensile and compressive strengths. An apparent elastic-viscous-plastic damage model is developed
and dolomite-induced deterioration mechanisms are investigated using computed tomography (CT) and scanning electron microscopy (SEM). The results indicate that: 1) Dolomite content enhances particle roundness
weakens intergranular interlocking
and creates distinct boundary pores with calcite
leading to enhanced pore connectivity and a 2.77-fold increase in porosity. 2) Dolomite presence reduces maximum tensile strain
decreases compressive strength by 14.5%
extends the compaction phase by 9%
and shortens the stable crack propagation phase by 12%. 3) A larger cyclic loading-unloading difference correlates with higher damage values. Dolomite-free rocks exhibit significant damage variation
with rapid early-stage increases followed by slower growth
whereas dolomite-containing rocks show more stable damage progression
with dolomite inducing more pronounced elastic-viscous-plastic damage accumulation. 4) Cracks in dolomite-free samples are bent
dissipating more energy with lower energy storage values
while those in dolomite-containing samples are straight
dissipating less energy with higher energy storage values. Dolomite enhances porosity
facilitating crack propagation and increasing the proportion of tensile cracks.