PAHs in Soil Determination by Ultrasonic Extraction and Gas Chromatography-Mass Spectrometry
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PAHs in Soil Determination by Ultrasonic Extraction and Gas Chromatography-Mass Spectrometry
Vol. 40, Issue 4, Pages: 10-14(2021)
作者机构:
国网河北省电力有限公司电力科学研究院
作者简介:
基金信息:
DOI:
CLC:X833;O657.63
Published:2021
稿件说明:
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CHE Kai, ZHOU Huibo, GONG Yunqian, et al. PAHs in Soil Determination by Ultrasonic Extraction and Gas Chromatography-Mass Spectrometry[J]. 2021, 40(4): 10-14.
DOI:
CHE Kai, ZHOU Huibo, GONG Yunqian, et al. PAHs in Soil Determination by Ultrasonic Extraction and Gas Chromatography-Mass Spectrometry[J]. 2021, 40(4): 10-14.DOI:
PAHs in Soil Determination by Ultrasonic Extraction and Gas Chromatography-Mass Spectrometry
A method is described for determination of polycyclic aromatic hydrocarbons(PAHs) in soil by gas chromatography with ultrasonic extraction.The effects of different extraction methods
ultrasonic time and extraction times on the standard recovery were compared.Giving the optimized condition is as follow: 10.0 g of sample is extracted ultrasonically with 20 ml N-hexane: acetone(1+1
v/v) as extraction solvent for 15 min and 4 times.Linearity ranges of 16 PAHs are within 20.0~500 μg/L and detection limits were 0.26~0.54 μg/kg.Blank silica sand average recovery was 63.0%~117.3%
average relative standard deviation was 4.3%~12.5%
and soil samples average recovery was 76.3%~110.3%
average relative standard deviation was 5.1%~18.6%.The results showed that this method had good operability
detection limits and accuracy
is able to accurate qualitative and quantitative analysis of PAHs in soil.