Study on Solid State Preparation of Nanometer Zirconia

HUANG Yu-ping; HUANG Hui-min; ZHENG Yu-ying; TANG Yun; JIANG Zhi-jian

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Study on Solid State Preparation of Nanometer Zirconia

更新时间：2026-05-27

- Study on Solid State Preparation of Nanometer Zirconia
- Vol. 24, Issue 3, Pages: 11-14(2007)
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- Published：2007
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黄玉萍, 黄慧民, 郑育英, 唐韵, 江志键. 固-化学反应制备纳米级氧化锆的工艺研究[J]. 广东工业大学学报, 2007, 24(3): 11-14.

HUANG Yu-ping, HUANG Hui-min, ZHENG Yu-ying, et al. Study on Solid State Preparation of Nanometer Zirconia[J]. 2007, 24(3): 11-14.
黄玉萍, 黄慧民, 郑育英, 唐韵, 江志键. 固-化学反应制备纳米级氧化锆的工艺研究[J]. 广东工业大学学报, 2007, 24(3): 11-14. DOI：

HUANG Yu-ping, HUANG Hui-min, ZHENG Yu-ying, et al. Study on Solid State Preparation of Nanometer Zirconia[J]. 2007, 24(3): 11-14. DOI：

摘要

采用氯氧化锆和草酸为原料进行低热固相反应

从而得到草酸氧锆前驱物

前驱物经煅烧得到纳米级ZrO2粉体.对前驱物进行了TG-DSC分析

对球磨条件、焙烧条件及其对产物粒径的影响进行探讨

并对分解产物进行XRD测定和TEM扫描.结果表明:产物粒度分布均匀

无明显团聚现象

纯度高

得到四方相为主的纳米氧化锆粉体

其平均粒径在11 nm左右.

Abstract

A new method to prepare ZrO2 nanoparticles is described.Precursors of ZrO2 were synthesized by solid state reaction of ZrOCl2·8H2O to C2H2O4·2H2O.Precursors were characterized by TG/DSC and the properties of zirconia were studied with aids of XRD

TEM.The effect of grinding and calcination on crystal was also investigated.The result shows that ultrafine zirconia with average particle size of 11nm has high purity and even distribution

and the main phase of the powder is tetragonal phase.

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references

冯长根,张江山,王亚军. 低温合成纳米级固溶体Ce1-xZrxO2的研究[J]. 硅酸盐学报. 2004(04)

夏宇正,朱也莉,石淑先,焦书科. 纳米二氧化锆的制备及其光学性能研究[J]. 涂料工业. 2006(08)

周新木,赵光好,谈宏宇,徐招弟,李炳伟. 纳米氧化锆的固相合成及机理研究[J]. 有色金属(冶炼部分). 2006(01)

吴文伟,廖森,姜求宇,宋宝玲,黎子学,邓广金. 室温固相反应法制备纳米氧化锆及表征[J]. 稀有金属. 2005(04)

黄传勇,唐子龙,张中太,金苗,陈清明. 氧化锆超细粉的绿色合成及粉末性能表征[J]. 材料工程. 2000(08)

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