STUDY ON HIGH-TEMPERATURE COMBUSTION MICROCOULOMETRIC METHOD FOR DETECTING THE CHLORINE CONTENT IN FIRE-RESITANT OIL

MING Julan; PAN Zhiying; ZHOU Feimei Zhejiang Provincial Electric Power Testing & Research Institute

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STUDY ON HIGH-TEMPERATURE COMBUSTION MICROCOULOMETRIC METHOD FOR DETECTING THE CHLORINE CONTENT IN FIRE-RESITANT OIL

更新时间：2025-09-28

- STUDY ON HIGH-TEMPERATURE COMBUSTION MICROCOULOMETRIC METHOD FOR DETECTING THE CHLORINE CONTENT IN FIRE-RESITANT OIL
- Thermal Power Generation Vol. 40, Issue 8, Pages: 30-33(2011)
- 作者机构：
  
  浙江省电力试验研究院
- 作者简介：
- 基金信息：
- DOI：
  CLC： TM621.8
- Published：2011
- 稿件说明：
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MING Julan, PAN Zhiying, ZHOU Feimei Zhejiang Provincial Electric Power Testing & Research Institute. STUDY ON HIGH-TEMPERATURE COMBUSTION MICROCOULOMETRIC METHOD FOR DETECTING THE CHLORINE CONTENT IN FIRE-RESITANT OIL[J]. Thermal power generation, 2011, 40(8): 30-33.
DOI：

MING Julan, PAN Zhiying, ZHOU Feimei Zhejiang Provincial Electric Power Testing & Research Institute. STUDY ON HIGH-TEMPERATURE COMBUSTION MICROCOULOMETRIC METHOD FOR DETECTING THE CHLORINE CONTENT IN FIRE-RESITANT OIL[J]. Thermal power generation, 2011, 40(8): 30-33. DOI：

摘要

介绍采用高温燃烧微库仑法检测抗燃油氯含量的原理

并进行了检测条件优化试验

得出转化率与主要影响因素如温度、增益、取样电阻、载气流速、氧气流速、偏压、进样量等的关系。在优化试验得出的最佳试验条件下对高温燃烧微库仑法进行了重复性测试和回收率测试

结果表明高温燃烧微库仑法检测抗燃油氯含量具有精密度和准确度高、分析速度快、干扰少、仪器设备费用少、维护工作量小等优点。

Abstract

The principle of adopting high-temperature combustion microcoulometric(HTCM) method for detecting chlorine content in fire-resistant oil

as well as optimization test of detecting conditions have been presented

the relationship between transformation rate and main affecting factors

namely temperature

gain

sample resistance

flow velocity of carrier gas

flow velocity of oxygen

biasing voltage

and sample intaking quantity etc.

being obtained.Under optimal test condition obtained from optimization test

test on repeatability and recovery rate of HTCM method has been carried out

results show that the HTCM method has many advantages

such as high precision and accuracy

papid anaysis velocity

few interference

low expense for instruments and equipment

little maintenance work etc..

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